[Course] 6th CERMAX practical course on basic NMR
When |
24 Jun, 2013 09:00 AM
to
27 Jun, 2013 06:00 PM |
---|---|
Where | ITQB |
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6th CERMAX practical course on basic NMR
The course is open and free of charge for NMR network members but practical sessions are restricted to 12 students. To apply please send an e-mail to lamosa@itqb.unl.pt stating your interest accompanied by a short CV.
Program
24th of June | ||
9.30 | Introduction to NMR spectroscopy (the phenomenon, basic properties of the signal) | |
10.30 | Instrumental aspects of the spectrometer /Rules for spectrometer use. | |
11.00 | Break | |
11.30 | Introduction to TopSpin software | |
12.00 | 1D Acquisition and processing | |
13.00 | Lunch break | |
14.00 | NMR and Metabolomics/ Quantitative NMR | |
15.30 | Break | |
16.00 | Spectrometer Guided tour and sample preparation | |
25th of June | ||
9.30 | Introduction to 2D NMR spectroscopy (Homonuclear correlation) | |
10.15 | INEPT, HSQC and HMBC | |
11.00 | Break | |
11.30 | Practical session I | |
Acquisition (1D, presat, p90, APT) Processing and analyzing 1D | ||
13.30 | Lunch break | |
14.30 | Practical sessions I (cont) | |
26th of June | ||
9.00 | The Nuclear Overhauser Effect | |
9.45 | The paramagnetic effect and metalloproteins | |
10.30 | Break | |
11.00 | Protein structure | |
11.45 | Practical session II | |
Acquisition (COSY, HSQC) Processing and analyzing 2D | ||
13.30 | Lunch break | |
14.30 | Practical sessions II (cont) | |
27th of June | ||
10.00 | Assignment strategies in small molecules (tutorial and exercises) | |
11.00 | Break | |
11.30 | Assignment strategies (cont) | |
13.00 | Lunch break | |
14.00 | Practical session III | |
Acquisition exercises |
Faculty
- Helena Matias
- Ivo Saraiva
- Luís Gafeira
- Manolis Matzapetakis
- Pedro Lamosa
- Ricardo Louro