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[Course] 7th CERMAX practical course on basic NMR

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When 24 Jun, 2014 09:30 AM to
27 Jun, 2014 05:00 PM
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7th CERMAX practical course on basic NMR

The course is open and free of charge for NMR network members, however the practical sessions are restricted to 12 students. To apply to this course please send an e-mail to lamosa@itqb.unl.pt stating your interest accompanied by a short CV until the 7th of June.

 

Program

24th of June
9.30   Introduction to NMR spectroscopy
10.30   Instrumental aspects of the spectrometer /Rules for spectrometer use.
11.00   Break
11.30   Introduction to TopSpin software
12.15   1D Acquisition and processing
13.00   Lunch break
14.00   NMR and Metabolomics/ Quantitative NMR
15.30   Break
15.50   Spectrometer Guided tour and sample preparation
     
25th of June
9.30   Introduction to 2D NMR spectroscopy (Homonuclear correlation)
10.15   Heteronuclear correlation for small molecule and protein assignment
11.00   Break
11.15   Practical session I
    Acquisition (1D, presat, p90, APT) Processing and analyzing 1D
13.30   Lunch break
14.30   Practical sessions I (cont)
     
26th of June
9.30   The Nuclear Overhauser Effect
10.15   The paramagnetic effect and metalloproteins
10.45   Break
11.15   Practical session II
    Acquisition (COSY, HSQC) Processing and analyzing 2D
13.30   Lunch break
14.30   Practical sessions II (cont)
     
27th of June
9.30   Assignment strategies in small molecules (tutorial and exercises)
 10.45   Break
 11.15   Assignment strategies (cont)
 13.00   Lunch break
14.00   Practical session III
    Acquisition exercises

Print program (pdf)


 
Faculty

  • Gonçalo Graça
  • Helena Matias
  • Ivo Saraiva
  • Manolis Matzapetakis
  • Pedro Lamosa
  • Ricardo Louro

 

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